Effect of Wet Spinning Parameters on Bamboo Cellulose Nanofiber Filament Preparation
نویسندگان
چکیده
Cellulose nanofibers (CNF) are materials synthesized from wood-based fibers having excellent mechanical properties due to their high crystallinity. In this research, the cellulose were bamboo fibers, as abundant natural available worldwide. The had been using chemical processes of bleaching with acetic acid and sodium chloride, followed by alkaline treatment hydroxide, hydrolysis sulfuric combined process in ultrasonic bath. Isolation nanocellulose scrap raw material was confirmed different analysis methods. morphology CNF characterized a scanning electron microscope (SEM). Fourier transform infrared spectrometer (FT-IR) X-Ray Diffractometer (XRD) examined structure identified crystallinity materials. monofilament prepared wet spinning process. effects coagulating solvent, water, methanol, acetone, calcium chloride (CaCl2) on formation studied. Morphology study carried out digital camera observe spinnability relationship conditions. thermal spun methanol acetone coagulation solvent analyzed differential calorimeter (DSC) thermogravimetric (TGA). Also, measuring degradation temperature compared extracted.
منابع مشابه
Fabrication of κ-Carrageenan Fibers by Wet Spinning: Spinning Parameters
This study demonstrates the fabrication of κ-carrageenan fibers by a wet-spinning method and discusses three important spinning parameters: coagulation bath composition, spinning rate and post-spinning mechanical drawing. The as-spun fiber diameter decreased with KCl and ethanol concentration in the coagulation bath. In general, the ultimate tensile stress and elongation at break both increased...
متن کاملPreparation and Characterization of Cellulose Nanocrystals from Bamboo Pulp
Cellulose nanocrystals (CNCs) can be obtained from bamboo pulp by hydrolysis with sulfuric acid. Firstly, the authors conducted a series of experiments under different conditions, and concluded that the optimal parameters were as follows: sulfuric acid concentration 60%, temperature 45 °C, the time is 90 minutes and the solid-liquid ratio is 1:8. Then, transmission electron microscopy (TEM), Fo...
متن کاملEffect of Melt Spinning Variables on the Structural Changes of Recycled and Bottle Grade Filament Yarn PET
متن کامل
effect of oral presentation on development of l2 learners grammar
this experimental study has been conducted to test the effect of oral presentation on the development of l2 learners grammar. but this oral presentation is not merely a deductive instruction of grammatical points, in this presentation two hypotheses of krashen (input and low filter hypotheses), stevicks viewpoints on grammar explanation and correction and widdowsons opinion on limited use of l1...
15 صفحه اولNanofiber assembly by rotary jet-spinning.
High-voltage electrical fields and low production rate limit electrospinning, the electrical charging of polymer liquids, as a means of nanofiber fabrication. Here, we show a facile method of fabrication of aligned three-dimensional nanofiber structures by utilizing high-speed, rotating polymer solution jets to extrude fibers. Termed rotary jet-spinning, fiber morphology, diameter, and web poro...
متن کاملذخیره در منابع من
با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید
ژورنال
عنوان ژورنال: Suan Sunandha Rajabhat University Journal of Science and Technology
سال: 2022
ISSN: ['2351-0889']
DOI: https://doi.org/10.53848/ssstj.v9i2.238